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host: ESRF / ID10-SURF, Oleg Konovalov
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ID10 consists fo two experimental stations: ID10-SURF / ID10-COH. Manageed by two teams, and the beamtime is shared in 50-50 mode
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ID: U35 + revolver U35/U27 + U27, 1.5m each
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optics
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- high heatload H-deflecting double mirrors, vertical deflecting DCM with channel cut Si111 (or Si311 for high resolution)
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- 4:1 Be 2D lens, R300 -> 10um v x 35um h in SURF hutch, 1D lens to come
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- (optional) vertical deflecting mirror
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- 11:1 Be 2D lens -> 2um v beam
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SURF hutch ~ 41m from ID
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- Double Xtal deflector (DCD), surface scattering (vertical stage unmounted)
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- 4.3m 2nd detector portal, horizontally rotatable
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10^13ph/s at 200mA, 10um v x 35um h beam, standard 22keV
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Experimental techniques:
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XRR/GIXRD/GISAXS/GIWAXS/XRF/XANES
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special: XRR with DCD using 333+660 to reach qz = 7.5/A (https://doi.org/10.1107/S1600576724000657)
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liquid surface XANES
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- using 4:1 lens, vertical deflecting mirror, no DCD, scan DCM but fix undulator gap (good for +/-100eV)
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- for different energies: set the 2/3 undulator set differently for different energy
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sample environments / experiment:
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- Langmuir trough
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- liquid-liquid Langmuir trough
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- liquid-liquid chamber
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- LMCats chamber from Leiden for 2D material CVD on liquid metal
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- humidity chamber
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- high pressure CO2 chamber (120bar)
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data (with Maciej Jankowski):
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- pipeline to XRR (ORSO format), GIXS / azimuthal integration
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- GIXS pipeline uses pyFAI fiberintegration
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- machine learning XRR (Schreiber's group)
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beamtime share:
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7 weeks / 6 months, 50% on liquid surface using DCD (mostly Langmuir trough and also LMCats)
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1.2 paper / proposal
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Coherence application: liquid-surface XPCS (Amadei, Journal of Physical Chemistry B, 124 (2020))
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